{"id":1511825,"date":"2019-11-29T13:47:24","date_gmt":"2019-11-29T05:47:24","guid":{"rendered":"https:\/\/www.bihec.com\/omnical\/?p=1511825"},"modified":"2019-11-29T13:47:24","modified_gmt":"2019-11-29T05:47:24","slug":"darc-%e7%9c%9f%e6%ad%a3%e7%9a%84%e7%bb%9d%e7%83%ad%e9%87%8f%e7%83%ad%e4%bb%aasupercrc%e5%8f%8d%e5%ba%94%e9%87%8f%e7%83%ad%e4%bb%aa%e7%be%8e%e5%9b%bdomnical-supercrc%e5%8f%8d%e5%ba%94%e9%87%8f","status":"publish","type":"post","link":"https:\/\/www.bihec.com\/omnical\/darc-%e7%9c%9f%e6%ad%a3%e7%9a%84%e7%bb%9d%e7%83%ad%e9%87%8f%e7%83%ad%e4%bb%aasupercrc%e5%8f%8d%e5%ba%94%e9%87%8f%e7%83%ad%e4%bb%aa%e7%be%8e%e5%9b%bdomnical-supercrc%e5%8f%8d%e5%ba%94%e9%87%8f\/","title":{"rendered":"DARC \u771f\u6b63\u7684\u7edd\u70ed\u91cf\u70ed\u4eea,SuperCRC,\u53cd\u5e94\u91cf\u70ed\u4eea,\u7f8e\u56fdOmnical SuperCRC\u53cd\u5e94\u91cf\u70ed\u4eea,\u5fae\u53cd\u5e94\u91cf\u70ed\u4eea ,\u5fae\u91cf\u70ed\u4eea ,\u7b49\u6e29\u91cf\u70ed\u4eea ,\u9ad8\u538b\u53cd\u5e94\u5fae\u91cf\u70ed\u4eea, \u9ad8\u538b\u53cd\u5e94\u91cf\u70ed\u4eea,"},"content":{"rendered":"

\"\"<\/p>\n

SuperCRC<\/a>\u662f\u4e00\u79cd\u5c0f\u578b\u7684\u53cd\u5e94\u91cf\u70ed\u4eea<\/a>\uff0c\u4e13\u4e3a\u5316\u5b66\u5de5\u827a\u5f00\u53d1\uff0c\u53cd\u5e94\u5de5\u7a0b\u653e\u5927\uff0c\u7269\u7406\u6027\u8d28\u6d4b\u91cf\u548c\u53cd\u5e94\u5371\u9669\u6027\u8bc4\u4f30\u800c \u8bbe\u8ba1\u3002\u8be5\u7cfb\u7edf\u53ef\u6d4b\u91cf\u5e7f\u6cdb\u7684\u70ed\u6548\u5e94\uff0c\u5e76\u4e3a\u5316\u5b66\u53cd\u5e94\u5de5\u7a0b\u653e\u5927\u63d0\u4f9b\u70ed\u529b\u5b66\u52a8\u529b\u5b66\u7b49\u53ef\u653e\u5927\u7684\u53c2\u6570\uff0c\u5305\u62ec\uff1a\u6700\u5927\u653e \u70ed\u91cf\u548c\u653e\u70ed\u901f\u7387\uff0c\u771f\u5b9e\u53cd\u5e94\u52a8\u529b\u5b66\u548c\u70ed\u529b\u5b66\uff0c\u6837\u54c1\u70ed\u5bb9\uff0c\u8f6c\u5316\u7387\u3002
\nSuperCRC\u80fd\u591f\u5728\u9ad8\u538b\uff0c\u53d8\u901f\u6405\u62cc\uff0c\u63a7\u5236\u6216\u6dec\u706b\u51b7\u5374\u548c\u89c6\u89c9\u89c2\u5bdf\u4e0b\u8fdb\u884c\u5b9a\u91cf\u7ed9\u6599\u548c\u6df7\u5408\uff0c\u4f7f\u5316\u5b66\u5bb6\u80fd\u591f\u6a21\u62df\u5404 \u79cd\u6df7\u5408\u548c\u53cd\u5e94\u8fc7\u7a0b\uff0c\u5e76\u8868\u5f81\u9884\u671f\u6216\u610f\u5916\u7684\u53cd\u5e94\u4e8b\u4ef6\u3002 SuperCRC\u91c7\u7528OmniCal\u4e13\u6709\u7684\u9884\u70ed\u52a0\u6837\u8bbe\u8ba1\uff0c\u6709\u52a9\u4e8e
\u52a0\u901f<\/a>\u6837\u54c1\u4e4b\u95f4\u7684\u70ed\u5e73\u8861\uff0c\u5e76\u6d88\u9664\u6837\u54c1\u6d4b\u8bd5\u8bef\u5dee\u3002<\/p>\n

\u53cd\u5e94\u5668<\/strong><\/p>\n

15ml\u5c0f\u74f6\u7528\u4f5c\u6807\u51c6\u73bb\u7483\u53cd\u5e94 \u5668\u3002\u8fd9\u4e9b\u5c0f\u74f6\u53ef\u4ee5\u914d\u5907\u5185\u90e8\u78c1 \u529b\u6216\u9876\u90e8\u6405\u62cc\u3002 \u9ad8\u538bHastelloyC\u53cd\u5e94\u5668\u53ef\u7528 \u4e8e\u9ad8\u8fbe3000psi\u7684\u538b\u529b\u53cd\u5e94.<\/p>\n

\u5de5\u4f5c\u8303\u56f4<\/strong><\/p>\n

SuperCRC\u7cfb\u7edf\u672c\u8eab\u53ef\u5728\u6e29\u81f3200\u2103\u4e4b\u95f4\u5347\u6e29\u548c\u6052\u6e29\u3002 \u4f7f\u7528\u4f4e\u6e29\u6052\u6e29\u5668<\/a>\uff0c\u7cfb\u7edf\u53ef\u4ee5\u5728 \u4f4e\u81f3-80\u2103\u7684\u6e29\u5ea6\u4e0b\u8fdb\u884c\u53cd \u5e94\u3002\u76ee\u524d\u6240\u6709SuperCRC\u90fd\u6709 \u91d1\u5c5e\u5185\u5faa\u73af\u7ba1\u8def\uff0c\u53ef\u4e0e\u4efb\u4f55\u7c7b \u578b\u7684\u4f20\u70ed\u4f20\u5bfc\u6d41\u4f53\u914d\u5408\u4f7f\u7528.<\/p>\n

\u8ddf\u8e2a\u53cd\u5e94<\/strong><\/p>\n

\u6211\u4eec\u7684\u7cfb\u7edf\u53ef\u5b9e\u65f6\u63d0\u4f9b\u70ed\u6d41\u91cf \u4fe1\u606f\uff0c\u53ef\u8f6c\u5316\u4e3a\u53ef\u653e\u5927\u7684\u70ed\u529b \u5b66\u548c\u52a8\u529b\u5b66\u53c2\u6570\u3002\u8bb0\u5f55\u7684\u5176\u4ed6 \u4fe1\u606f\u5305\u62ec\u6e29\u5ea6\uff0c\u538b\u529b\uff0c\u5242\u91cf \uff08\u9700\u8981\u6ce8\u5c04\u6cf5\uff09\u548c\u53cd\u5e94\u8f6c\u5316\u7387 \u66f2\u7ebf\u7b49\u3002<\/p>\n

\u53cd\u5e94\u5668<\/strong><\/p>\n

\u5bb9\u5668\u5bb9\u79ef\uff1a 15\u6beb\u5347\uff0c<\/p>\n

\u6700\u5c0f\u6837\u54c1\u5de5\u4f5c\u5bb9\u79ef\uff1a1\u6beb\u5347<\/p>\n

\u6df7\u5408\u80fd\u529b\uff1a 4\u4e2a<\/p>\n

\u9644\u52a0\u6216\u6cf5\u6ce8\u5c04\uff08\u73bb\u7483\u5bb9\u5668\uff09 1\u4e2a<\/p>\n

\u9644\u52a0\u6216\u6cf5\u6ce8\u5c04\uff08\u91d1\u5c5e\u5bb9\u5668\uff09<\/p>\n

\u6ce8\u5c04\u5668\u5927\u5c0f\uff1a \u5fae\u5347\uff0c1\u6beb\u5347\u548c3\u6beb\u5347\uff0c\u73bb\u7483\u6216\u4e00\u6b21\u6027\u5851\u6599<\/p>\n

\u6405\u62cc\u6a21\u5f0f\uff1a 0 ~ 1000 rpm\uff08\u6570\u5b57\u663e\u793a\uff0c\u78c1\u529b\u6405\u62cc\uff09<\/p>\n

\u5ba4\u538b\uff1a 0 ~ 1 bar\uff08\u73bb\u7483\u6df7\u5408\u5bb9\u5668\uff09 0 ~ 200 bar\uff08\u91d1\u5c5e\u6df7\u5408\u5bb9\u5668\uff09<\/p>\n

\u81ea\u52a8\u5378\u538b\uff1a 0 ~ 50 bar \u8d85\u538b<\/p>\n

\u6e29\u5ea6\uff1a -80 ~ +200 \u2103<\/p>\n

\u5347\u6e29\u901f\u7387\uff1a 0.1 ~ 3 \u2103\/min<\/p>\n

\u51b7\u5374\uff1a \u4f7f\u7528\u5916\u90e8\u4f4e\u6e29\u6052\u6e29\u5668\uff0c<\/p>\n

\u6700\u9ad8\u53ef\u8fbe -2 \u2103\/min \u76ee\u89c6\u68c0\u67e5\uff1a \u901a\u8fc7\u5185\u7aa5\u955c\u76ee\u89c6\u68c0\u67e5<\/p>\n

\u91cf\u70ed\u8ba1 <\/strong><\/p>\n

\u6a21\u5f0f\uff1a \u7b49\u6e29\u548cDSC<\/a>\u6a21\u5f0f<\/p>\n

\u7cbe\u5ea6\uff1a 1 mcal\u62161\uff05\u7684\u6d4b\u91cf<\/p>\n

\u70ed\u7075\u654f\u5ea6\uff1a \u00b11\u03bcW\uff0c\u9759\u6b62<\/p>\n

\u00b120\u03bcW\uff0c\u00a0\u78c1\u529b\u6405\u62cc<\/p>\n

\u00b120\u03bcW\uff0c\u673a\u68b0\u6405\u62cc<\/p>\n

\u65f6\u95f4\u5e38\u6570\uff1a 1.3\u81f32.3\u5206\u949f\uff08\u7531\u6a21\u578b\u51b3\u5b9a\uff09<\/p>\n

\u52a8\u6001\u6821\u6b63\uff1a \u5185\u7f6e\u52a8\u6001\u6821\u6b63\u529f\u80fd<\/p>\n

\u7535\u6e90\u8981\u6c42\uff1a 120 VAC\uff0c50-60 Hz\uff08220 VAC\u53ef\u9009\uff09<\/p>\n

\u5c3a\u5bf8\uff1a 20″ \u9ad8 x 16″ \u5bbd x 15″ \u6df1\uff0851cmx 41cmx 38cm\uff09<\/p>\n

\u4fe1\u53f7\u8f93\u51fa\u7aef\u53e3\uff1a \u80fd\u591f\u68c0\u6d4b\u538b\u529b\u6216\u8005\u8d28\u91cf\u6d41<\/p>\n

\u8f6f\u4ef6 <\/strong><\/p>\n

WinCRC\uff1a \u5728\u5fae\u8f6fWindows 7\uff0c10\u4e0a\u5177\u6709\u76f4\u89c2\u7684\u56fe\u5f62\u7528\u6237\u754c\u9762<\/p>\n

\u53ef\u9009\u8bbe\u5907<\/strong><\/p>\n

\u538b\u529b\u5305\uff1a \u4e0d\u9508\u94a2\u54c8\u6c0f\u5408\u91d1\u538b\u529b\u5bb9\u5668\u5957\u4ef6\uff0c\u7535\u78c1\u5b89\u5168\u9600\u548c\u7279\u6c1f\u9f99\u5bc6\u5c01\u4ef6\u3002 \u6709\u4e0d\u540c\u7684\u6ce8\u5c04\u53e3\u914d\u7f6e\uff0c\u8bf7\u8054\u7cfbOmnical<\/a>\u4e86\u89e3\u66f4\u591a\u4fe1\u606f\u3002 \u6ce8\u5c04\u6cf5\uff1a \u53cc\u91cd\u8f93\u6db2\u6216\u6ce8\u5165\/\u62bd\u51fa\u5355\u5143 \u9876\u7f6e\u5f0f\u6405\u62cc\u5668\uff1a \u9ad8\u626d\u77e9\u53d8\u901f\u9876\u7f6e\u5f0f\u6405\u62cc\u5668\uff0c HastelloyC\u6405\u62cc\u8f74\u548cTeflon\u53f6\u8f6e\u3002<\/p>\n

\u5e94\u7528 <\/strong><\/p>\n

\u25ce\u53cd\u5e94\u70ed<\/a><\/p>\n

\u25ce\u53cd\u5e94\u52a8\u529b\u5b66<\/p>\n

\u25ce\u70ed\u5bb9\u91cf<\/p>\n

\u25ce\u5316\u5b66\u7a33\u5b9a\u6027<\/p>\n

\u25ce\u540c\u6e90- \u591a\u76f8\u50ac\u5316<\/p>\n

\u25ce\u6c14\u4f53\u5438\u9644<\/p>\n

\u25ce\u7ed3\u6676<\/p>\n

\u25ce\u6eb6\u89e3<\/p>\n

\u25ce\u4e2d\u548c<\/p>\n

\u25ce\u805a\u5408<\/p>\n

\u25ce\u53cd\u5e94\u4f18\u5316<\/p>\n

\u53c2\u8003\u6587\u732e <\/strong><\/p>\n

Detection and Elimination of Product Inhibition from the Asymmetric Catalytic Hydrogenation of Enamines Karl B. Hansen,*, Thorsten Rosner,*, Michele Kubryk,Peter G. Dormer, and, and Joseph D. Armstrong, III Organic Letters 2005 7 (22), 4935-4938 DOI: 10.1021\/ol051862d Chiral Phosphine Olefin Ligands in the Rhodium-Catalyzed Asymmetric 1,4-Addition Reactions Wei-Liang Duan,, Hiroshi Iwamura,, Ryo Shintani,*, and, and Tamio Hayashi*, Journal of the American Chemical Society 2007 129 (7), 2130-2138 DOI: 10.1021\/ja0671013 Mechanistic Insight<\/a>s into the Pd(BINAP)-Catalyzed Amination of Aryl Bromides: Kinetic Studies under Synthetically Relevant Conditions Utpal K. Singh,, Eric R. Strieter,, Donna G. Blackmond,*, and, and Stephen L. Buchwald*, Journal of the American Chemical Society 2002 124 (47), 14104-14114 DOI: 10.1021\/ja026885r<\/p>\n

DARC \u771f\u6b63\u7684\u7edd\u70ed\u91cf\u70ed\u4eea<\/a>\nSuperCRC<\/a>\n\u53cd\u5e94\u91cf\u70ed\u4eea<\/a>\n\u5fae\u53cd\u5e94\u91cf\u70ed\u4eea<\/a>\n\u5fae\u91cf\u70ed\u4eea<\/a>\n\u7b49\u6e29\u91cf\u70ed\u4eea<\/a>\n\u7f8e\u56fdOmnical SuperCRC\u53cd\u5e94\u91cf\u70ed\u4eea<\/a>\n\u9ad8\u538b\u53cd\u5e94\u5fae\u91cf\u70ed\u4eea<\/a>\n\u9ad8\u538b\u53cd\u5e94\u91cf\u70ed\u4eea<\/a><\/div>","protected":false},"excerpt":{"rendered":"

SuperCRC\u662f\u4e00\u79cd\u5c0f\u578b\u7684\u53cd\u5e94\u91cf\u70ed\u4eea\uff0c\u4e13\u4e3a\u5316\u5b66\u5de5\u827a\u5f00\u53d1\uff0c\u53cd\u5e94\u5de5\u7a0b\u653e\u5927\uff0c\u7269\u7406\u6027\u8d28\u6d4b\u91cf\u548c\u53cd\u5e94\u5371\u9669\u6027\u8bc4\u4f30\u800c \u8bbe\u8ba1\u3002\u8be5\u7cfb\u7edf\u53ef\u6d4b\u91cf\u5e7f\u6cdb\u7684\u70ed\u6548\u5e94\uff0c\u5e76\u4e3a\u5316\u5b66\u53cd\u5e94\u5de5\u7a0b\u653e\u5927\u63d0\u4f9b\u70ed\u529b\u5b66\u52a8\u529b\u5b66\u7b49\u53ef\u653e\u5927 <\/p>\n","protected":false},"author":22,"featured_media":1511769,"comment_status":"open","ping_status":"open","sticky":false,"template":"","format":"standard","meta":[],"categories":[3],"tags":[50,5,10,8,9,11,51,12,37],"_links":{"self":[{"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/posts\/1511825"}],"collection":[{"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/posts"}],"about":[{"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/types\/post"}],"author":[{"embeddable":true,"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/users\/22"}],"replies":[{"embeddable":true,"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/comments?post=1511825"}],"version-history":[{"count":1,"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/posts\/1511825\/revisions"}],"predecessor-version":[{"id":1511827,"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/posts\/1511825\/revisions\/1511827"}],"wp:featuredmedia":[{"embeddable":true,"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/media\/1511769"}],"wp:attachment":[{"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/media?parent=1511825"}],"wp:term":[{"taxonomy":"category","embeddable":true,"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/categories?post=1511825"},{"taxonomy":"post_tag","embeddable":true,"href":"https:\/\/www.bihec.com\/omnical\/wp-json\/wp\/v2\/tags?post=1511825"}],"curies":[{"name":"wp","href":"https:\/\/api.w.org\/{rel}","templated":true}]}}