Harrick Praying Mantis 螳螂™ 高溫反應(yīng)室對(duì)于具有高比表面積的粉末特別有效。這使得漫反射成為研究多相催化、氣固相互作用、光化學(xué)反應(yīng)和氧化機(jī)制的有價(jià)值的工具。這種高溫反應(yīng)室非常適合在精心控制的溫度和壓力下進(jìn)行此類研究。高溫反應(yīng)室應(yīng)用允許在受控壓力和廣泛溫度下進(jìn)行漫反射(漂移)光譜測量。它和螳螂一起使用™ 紅外光譜和紫外-可見漫反射光譜的附件。也可用于拉曼光譜。
特征
設(shè)計(jì)用于從高真空(133μPa或10-6torr)到133kpa(1ktorr),帶KBr窗口或1.5mpa(11.3ktorr)帶ZnSe窗口的操作。
達(dá)到910°C的溫度(在真空下)。
易于適應(yīng)高達(dá)3.44MPa(25.8ktorr)的操作,帶有可選的高壓圓頂。
提供三個(gè)入口/出口,用于排空電池和引入氣體。
由耐化學(xué)腐蝕的316不銹鋼制成。
可選的Silcotek/Restek惰性涂層可提高惰性和耐腐蝕性。
可選的冷卻筒可用于中等程度的冷卻或加熱,帶有冷卻器或再循環(huán)裝置。
可用于顯微光譜應(yīng)用的替代窗口組件,包括拉曼。
包括
反應(yīng)室。
低壓加熱筒。
K型熱電偶。
樣品包裝工具和溢液盤。
帶有兩個(gè)KBr或ZnSe窗口和一個(gè)玻璃觀察窗口(FTIR配置)的圓頂。
帶有兩個(gè)SiO2窗口和一個(gè)玻璃觀察窗口(UV-Vis-NIR配置)的圓頂。
相關(guān)配件:
MODEL NO. | NAME | DESCRIPTION | |
---|---|---|---|
ATK-024-3 | Temperature Controller, 110V | Temperature Controller (110V) with USB to RS-485 Adapter | |
ATK-024-4 | Temperature Controller, 220/240V | Temperature Controller (220/240V) with USB to RS-485 Adapter | |
CHC-CHA-3 | Praying Mantis™ Low Temperature Reaction Chambers (FTIR) | Praying Mantis™ diffuse reflection environmental chamber, 24V | |
CHC-VUV-3 | Praying Mantis™ Low Temperature Reaction Chambers (UV-Vis-NIR) | Praying Mantis™ diffuse reflection environmental chamber, 24V | |
DRK-3-XXX | Diffuse Reflection Catalysis Package, 110V | Kit with Praying Mantis, Reaction Chamber, Controller, etc. | |
DRK-4-XXX | Diffuse Reflection Catalysis Package, 220V | Kit with Praying Mantis, Reaction Chamber, Controller, etc. | |
DRP-XXX | Praying Mantis™ Diffuse Reflection Accessory | Diffuse reflection accessory |
MODEL NO. | NAME | |
---|---|---|
007-085 | VCO to Swagelok Adapter (English) | |
116-998 | VCO to Swagelok Adapter (Metric) | |
DRP-ASC | Ambient Chamber (FTIR) for Praying Mantis | |
DRP-ASC-VUV | Ambient Chamber (UV-Vis-NIR) for Praying Mantis | |
DRP-PDR | Praying Mantis Purge Shield | |
HVC-COL | HVC Cooling Cartridge | |
HVC-DWA-2 | Standard Reaction Chamber Dome, SiO? | |
HVC-DWA-3 | High Press. Dome, SiO?, for High Temp. Chamber | |
HVC-DWI-2 | Standard Reaction Chamber Dome, ZnS | |
HVC-DWI-3 | High Press. Dome, ZnS, for High Temp. Chamber | |
HVC-DWM-2 | Standard Reaction Chamber Dome, ZnSe | |
HVC-DWM-3 | High Press. Dome, ZnSe, for High Temp. Chamber | |
HVC-DWP-2 | Standard Reaction Chamber Dome, KBr | |
HVC-MRA | Standard Reaction Chamber Raman Assembly, SiO? |
易耗配件:
MODEL NO. | NAME | ||
---|---|---|---|
008-144 | Thermocouple, K-Type | ||
116-439 | Screen Set (2 each of the three sizes), 6.3 mm dia. | ||
116-439-1S | Screen Set (6), pore size 0.104 mm (0.0041″), 6.3 mm dia. | ||
116-439-2S | Screen Set (6), pore size 0.061 mm (0.0024″), 6.3 mm dia. | ||
116-439-3S | Screen Set (6), pore size 0.038 mm (0.0015″), 6.3 mm dia. | ||
HVC-CER | Ceramic Filters (4, 80um max. pore dia), 6.3 mm dia. | ||
KIT-SCP | Spatula/Scoopula |
MODEL NO. | NAME | ||
---|---|---|---|
116-429 | PTFE Washer, OD 0.59″ (15mm) |
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MODEL NO. | NAME | ||
---|---|---|---|
HVC-ORK | Kalrez O-Rings for High Temp. Reaction Chambers | ||
HVC-ORV | Viton O-Rings for High Temp. Reaction Chambers | ||
ORK-010 | Kalrez O-Ring, 0.379 OD, 0.239 ID | ||
ORK-013 | Kalrez O-Ring, 0.566 OD, 0.426 ID | ||
ORK-016 | Kalrez O-Ring, 0.754 OD, 0.614 ID | ||
ORK-023 | Kalrez O-Ring, 1.191 OD, 1.051 ID | ||
ORV-010 | Viton O-Ring, 0.379 OD, 0.239 ID | ||
ORV-013 | Viton O-Ring, 0.566 OD (15 mm), 0.426 ID | ||
ORV-016 | Viton O-Ring, 0.754 OD, 0.614 ID | ||
ORV-023 | Viton O-Ring, 1.191 OD, 1.051 ID |
MODEL NO. | NAME | ||
---|---|---|---|
KBR-100 | KBr Powder, Spectroscopic Grade, 100 g |
MODEL NO. | NAME | ||
---|---|---|---|
WAD-U23 | Window SiO? 15 x 2 mm | ||
WAD-U43 | Window SiO? 15 x 4 mm | ||
WED-U23 | Window Si 15 x 2 mm | ||
WFD-U23 | Window CaF? 15 x 2 mm | ||
WHD-U23 | Window BaF? 15 x 2 mm | ||
WID-U43 | Window ZnS 15 x 4 mm | ||
WJD-U23 | Window Ge 15 x 2 mm | ||
WLD-U23 | Window NaCl 15 x 2 mm | ||
WMD-U23 | Window ZnSe 15 x 2 mm | ||
WMD-U43 | Window ZnSe 15 x 4 mm | ||
WPD-U23 | Window KBr 15 x 2 mm |